Abstract
The electron precise [Mo(3)(μ(3)-S)(μ-S)(3)(dppe)(3)Br(3)](+) incomplete cuboidal complex with six cluster skeletal electrons (CSE) can be converted to the paramagnetic bicapped [Mo(3)(μ(3)-S)(2)(μ-S)(3)(dppe)(3)](+) cluster with an unusual seven metal electron population by treatment with (t)BuSNa, which simultaneously serves as a reducing agent and a source of the additional capping sulfur atom.
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