Abstract
Reductive amination of the macrolide antibiotic josamycin with alkyl amines, using three different reducing agents: NaBH 3CN, NaBH 4 and NaBH(OAc) 3, yields surprisingly different major products which are identified as either Lewis complexes, aminoalkyl derivatives or α,β-unsaturated derivatives of josamycin by 1H and 13C NMR, FT-IR and ESI MS methods.
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