Abstract

IntroductionThe purpose of this study was to investigate the influence of both polymerization cycles and mechanical exposure procedures on the adhesion of instrument fragments using a modified tube technique with a light-curing composite. MethodsEighty Mtwo instruments (size 15.05; VDW, Munich, Germany) were cut at a diameter of 35/100 mm and clamped in a vice with an overlap of 2 mm. Matching cannulas were filled with SDR composite (Dentsply, York, PA) and placed over the instruments. Prime & Bond Active (Dentsply Sirona, Bensheim, Germany) was used as the bonding material. Glass fiber was inserted from the opposite side into the cannula, and 1, 2, 4, or 6 polymerization cycles of 30 seconds were applied (800 mW/mm2) (n = 20/group). Sixty further identical instruments (n = 20/group) were divided into the following groups: group 1, cut at 10 mm and left unprepared (taper = 5%); group 2, parallelized using diamond instruments (taper = 0%); and group 3, prepared in a way that an inverted conical taper resulted (taper = 2%). Polymerization was performed for 2 minutes. The failure load and mode of failure were determined using a tensile testing device (2 mm/min). Data were statistically analyzed using the Kruskal-Wallis or chi-square test. ResultsThe failure load increased significantly with the number of polymerization cycles (P < .0001). More than 4 polymerization cycles had no further benefit (P > .05). The failure load in the inverted conical group was significantly lower (P < .0001) compared with the parallel and the unprepared groups. Adhesive failure was significantly more frequent in groups 2 and 3 (20/20) than in group 1 (16/20) (P < .05). ConclusionsBoth the number of polymerization cycles and the mechanical exposure procedures had a significant impact on the adhesive force when using the tube technique.

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