Abstract
AbstractA synthetic method for the preparation of unsymmetrical 2‐arylthioacetamides though direct C(sp3)−H thiolation of arylacetamides with readily available substituted thiols, sulfenylchlorides and disulfides have been developed. Our strategy features a green reaction medium with ample substrate scope, affording the mono‐thiolated aryl acetic acid derivatives in moderate to good yields in the presence of weak bases without any transition‐metal catalyst.
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