Abstract
A new layered zinc phosphite, H(2)tmdp x Zn(3)(HPO(3))(4) (tmdp = 4,4'-trimethylenedipiperidine), was prepared in a flux of phosphorous acid without the addition of water as a solvent. The compound could be transformed into a new three-dimensional open-framework zinc phosphite, Zn(2)(H(2)O)(4)(HPO(3))(2) x H(2)O, with intersecting 16- and 12-ring channels at room temperature.
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