Track-Rex: A universal toolbox for tracking recrystallization nucleation and grain growth behaviors in polycrystalline materials

Abstract

Recrystallization annealing is widely used to tailor the microstructure and enhance the performance of cold-deformed metallic materials. However, the underlying recrystallization mechanisms are debated, even with the use of cutting-edge characterization techniques. Here, we develop a Track-Rex toolbox to analyze quasi-in-situ electron backscatter diffraction (EBSD) datasets of two magnesium (Mg) alloys during static recrystallization via grain correlation. The results show that the recrystallized grains do not always grow; instead, they can shrink or even be consumed. This is attributed to the presence of newly formed recrystallized grains that possess a growth advantage over the old recrystallized grains. The rare earth containing Mg-2.4Zn-0.2Ce wt.% (ZE20) alloy exhibits a higher nucleation activity in the shear bands compared to the commercial Mg-3Al-1 Zn (AZ31) alloy. Regardless of the nucleation timing and sites, recrystallized grains in the ZE20 alloy show consistent off-basal orientations, serving as the origin of the rare earth texture. Moreover, the off-basal texture of these recrystallized grains is further strengthened through preferential growth during subsequent annealing. On the contrary, the recrystallized grains in the AZ31 exhibit scattered basal orientations that grow uniformly, resulting in a weak basal texture.