Abstract
An ICP-AES based method was developed for the direct determination of precious metals without any chemical/physical separation in nuclear materials and it was found to be simple, sensitive, less time consuming, no organic waste generation and no need of selective extraction. Analytical performance including detection limits, sensitivity, linear dynamic range, precession of different analytical lines of these elements was studied alongwith the spectral interference of U, Th and Zr to choose the best analytical lines. EDXRF method was used for comparison purpose.
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