Toughening of a Particulate‐Reinforced Ceramic‐Matrix Composite by Thermal Residual Stress

Abstract

The micromechanics involved in increased crack growth resistance, KR, due to the addition of TiB2 particulate in a SiC matrix was analyzed both experimentally and theoretically. The fractography evidence, in which, the advancing crack was attracted to adjacent particulates, was attributed to the tensile region surrounding a particulate. Countering this effect is the compressive thermal residual stress, which results in the toughening of the composite, in the matrix. This thermal residual stress field in a particulate‐reinforced ceramic‐matrix composite is induced by the mismatch in the coefficients of thermal expansion of the matrix and the particulate when the composite is cooled from the processing to room temperature. The increase in KR of the composite over the monolithic matrix, which was measured by using a hybrid experimental‐numerical analysis, was 77%, and compared well with the analytically predicted increase of 52%. The increase in KR predicted by the crack deflection model was 14%. Dependence of KR on the volume fraction of particulates, fp, and of voids, fv, is also discussed.