Abstract
Build ‘em up and knock ‘em down: natural pinnaic acid and three of its stereoisomers were synthesized from the aldehydes described in the preceding communication. A key step in the synthesis of natural pinnaic acid was a highly stereoselective reduction of ketone 1. The stereochemistry was determined by means of degradation studies of the synthetic material; TBS=tert-butyldimethylsilyl.
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