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Abstract
The crystal structure of monoclinic thallium(III) hydrogendiphosphate, TlHP2O7, has been solved from laboratory X-ray powder diffraction data and refined by the Rietveld method. All atoms occupy general positions. The TlIII ions have a distorted octahedral coordination environment of O atoms from four diphosphate groups. Adjacent TlO6 octahedra form edge-shared Tl2O10 dimers which share corners with PO4 tetrahedra to build a three-dimensional polymeric structure.
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