Abstract

The indicator, diphenylaminesulfonic acid, is shown to be responsible for the disproportionality observed between milligrams of uranium titrated and milliliters of potassium dichromate used, when the titration end point is determined visually. Determining the end point potentiometrically, the discrepancy was eliminated within certain limits. and optimum conditions were found for the potentiometric titration of as little as 10 mg of uranium.

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