Abstract
Initial screening of the moderately volatile range of the tire fire oil prior to fractionation was performed using capillary gas chromatography with dual, simultaneous detection. Samples were analyzed with a postcolumn split to a flame ionization capture detector (FID) and an electron capture detector (ECD); no peaks were detected by the ECD. Using another system with the column split to an FID and a thermionic specific detector (TSD) sensitive to nitrogen- and phosphorus-containing compounds, several components were detected that were not evident in the complex FED chromatogram. The TSD-FID response data complemented the mass spectral data for identifications. 2 tables, 4 figures.
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