Abstract

An equiaxed, submicron grain size distribution was generated in an Al(0.1wt.% Sc) alloy by processing through equal channel angular pressing followed by a low temperature pre-ageing heat treatment. The alloy was subsequently annealed for various times at 300, 350, 400 and 450°C for investigating the thermal stability of the deformation microstructure. It was found that up to 400°C, the submicron grain structure coarsens slowly and uniformly by a process of continuous recrystallization. Within this temperature range, the uniform dispersion of nano-sized Al3Sc particles generated by the pre-ageing treatment substantially hinders grain coarsening by Zener pinning of the (sub)grain boundaries. At the higher annealing temperature of 450°C, certain grains were found to grow discontinuously thereby generating a mixed microstructure consisting of both fine and coarse grains. The data in this study was combined with recent data for a higher solute Al(0.3wt.% Sc) alloy for furthering our understanding of the time and temperature range in which this family of alloys is resistant to rapid, discontinuous grain coarsening (recrystallization).

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