Abstract
We present the fabrication of a three-dimensional (3D) assembly of flower-like Au structures via the combination of 3D macroporous Au-coated microspheres and surface nanoarchitectures using electrodeposition of nanoplate Au structures. The 3D flower-like Au structures exhibit synergistically enhanced electrocatalytic activities regarding glucose oxidation and oxygen reduction compared to those of the individual 3D macroporous and nanoplate Au structures. The 3D flower-like Au structures can also be utilized as electroanalytical platforms retaining the combined advantages of both of the 3D macroporous and nanoplate Au structures.
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