Abstract
Although the temperature window of helium ion irradiation for gas bubble superlattice (GBS) formation was found to be in the range of approximately 0.15–0.35 melting point in literature, the thermal stability of He GBS has not been fully investigated. This work reports the experiment using an in-situ heating holder in a transmission electron microscope (TEM). A 3.0 mm TEM disc sample of Mo (99.95% pure) was irradiated with 40 keV He ions at 300 °C to a fluence of 1.0E+17 ions/cm2, corresponding to a peak He concentration of approximately 10 at.%, in order to introduce He GBS. In-situ heating was conducted with a ramp rate of ∼25 °C/min, hold time of ∼30 min, and temperature step of ∼100 °C up to 850 °C (0.39Tm homologous temperature). The result shows good thermal stability of He GBS in Mo with no noticeable change on GBS lattice constant and ordering. The implication of this unique and stable ordered microstructure on mechanistic understanding of GBS and its advanced application are discussed.
Sign-in/Register to access full text options 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
