Abstract
Thermal dehydration and decomposition processes of some intercalation compounds were studied by simultaneous TG/DSC and evolved gas analysis (EGA). γ-Zirconium and γ-titanium phosphates were intercalated with 1,10-phenanthroline and subsequently reacted with copper ions to form the complex in situ. Reaction mechanisms for thermal decomposition of all the materials were investigated and proposed according to the mass losses recorded by TG and confirmed by EGA (TG–FTIR). The Ozawa–Flynn–Wall isoconversional method provided dependencies of activation energy on the degree of conversion. A “single point” model-free method was also applied using Kissinger equation and the derived results were compared to those of the former method.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
