Abstract
Partial decoupling and the INDOR technique are used to measure the nuclear magnetic resonance splittings that are small enough to be obscured by the magnet-field inhomogeneity; J BX = (0.10 ± 0.01) Hz in 2,3-dibromopropene. Double irradiation experiments at certain frequencies which produce sign dependent asymmetries are used to determine the magnitude and sign of the coupling constants in 2,3-dibromopropene.
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