Abstract
Two simple thermometric procedures have been applied to the quantitative analysis of Grignard reagents. In the first method the Grignard reagent was titrated with a standard solution of isopropyl alcohol and the end-point located by monitoring the temperature change. In the other method a single measurement of temperature was made after reacting the Grignard reagent with an excess of isopropyl alcohol. The maximum temperature reading was then referred to a temperature scale directly calibrated in concentration units.
Published Version
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