Abstract
The heating of Rh 6(CO) 16 absorbed on α-alumina to 400 °C in either He or h 2 gave primarily carbon monoxide resulting from the thermal decarbonylation of the cluster. A little CO 2 was also formed at higher temperatures in either He or H 2. At these higher temperatures under H 2 a small amount of CH 4 was also produced, but no evidence for the presence of higher hydrocarbons could be found.
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