Abstract
Thiathromboxane analogues (2) and (19) have been prepared by an extremely short and efficient synthetic route which can also be employed to make simple 2,3-dialkylated thian-4-ones. The cornerstone of the synthetic strategy is the organocopper conjugate addition – enolate alkylation reactions of 3-methoxycarbonyl-5,6-dihydrothiin-4-one (1b).
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