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Abstract
Abstract The conversion of racemic linalyl acetate to racemic lilac alcohols has been completed in 5 steps and four diastereoisomers of β,5-dimethyl-5-vinyl-2-tetrahydrofuranethanol were obtained. d-Lilac alcohols were also synthesized from d-linalyl acetate and confirmed to be identical with natural ones. The absolute configurations of lilac alcohol-a, -b, -c, and -d were respectively shown to be (βS, 2S, 5S), (βR, 2S, 5S), (βR, 2R, 5S), and (βS, 2R, 5S) by the chemical and physical evidences.
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