Abstract
1-methyl-3-butyl Imidazole chloride is prepared by 1–methyl imidazole and chlorinated n-butane. The synthesis reaction of 1-methyl-3-butyl imidazole tetrafluoroborate is in the acetone. The solubility of NaBF4and BMIC in acetone is not large, but due to the insolubility in acetone of reaction product NaCl and continuous precipitation from the liquid phase in the reaction process, so as to promote the reaction continuously towards forward direction. The colorless transparent and odorless BMIBF4are gotten. We use infrared spectrometer for the structure characterization, it is proved that we have gotten BMI-BF4room temperature ionic liquids. BMIC ionic liquid has better solubility in H2O, ethanol, ethyl acetate, acetone, acetonitrile, and methanol, and is insoluble in the ether and cyclohexane.
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