Abstract
A range of alkyl spacer-tethered 1,2- and 1,3-diols have been prepared from commercially available Merrifield resin ( 1 ) and (4-chloromethyl)phenylpentyl-polystyrene-co-divinylbenzene ( 2 ). The utility of these resin-bound diols as supports for the Ti(IV)-catalysed Diels–Alder reaction has been exemplified and it has been demonstrated that the length of the tether has a direct effect upon the catalytic activity.
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