Abstract
Zintlating stuff! The first binary Sn/Sb Zintl anions produced by solution techniques were obtained in [K([2.2.2]crypt)]2[Sn2Sb2]⋅en (en=ethylenediamine) and [K6(NH3)9][Sn3Sb4] upon extraction of K8SnSb4 by en or liquid ammonia. Addition of ZnPh2 to the en/[2.2.2]crypt extract resulted in the formation of a heterotrimetallic complex in [K([2.2.2]crypt)]3[Sn2Sb5(ZnPh)2]⋅en⋅0.5tol (see scheme).
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