Abstract

AbstractTetrakis(pentafluorophenyl)tellurium(IV), Te(C6F5)4, was prepared from the reaction of TeCl4 and Mg(C6F5)Br. Crystallization of the crude product from n‐pentane at −25 °C gave suitable single crystals. The title compound crystallizes in the monoclinic space group P21/c (Z = 8) with two independent molecules per unit cell.

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