Abstract
AbstractManganese(II) biphenyl-4,4′-dicarboxylate, prepared by crystallization of a mixture of biphenyl-4,4′- dicarboxylic acid, manganese(II) chloride, and di(4-pyridyl)acetylene as base in a mixture of dimethylformamide, ethanol and water in a closed vessel at elevated temperatures forms a 3D network of {[Mn(bpdc)(H2O)2][Mn(bpdc)(H2O)]} containing one five-fold coordinated and one six-fold coordinated Mn metal center (X-ray structure determination). Scanning tunneling microscopic (STM) measurements of manganese biphenyl-4,4′-dicarboxylate adsorbed on highly oriented pyrolytic graphite showed strands, the averaged diameter of which amounts to 18±1 nm, whereas the apparent height is about 0.5±0.02 nm.
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