Abstract
The crystal structure of H 3PMo 6W 6O 40 3C 2H 6O was determined by X-ray crystallography and refined to R = 0.0698 based on 2279 observed reflections to give unit cell parameters a = 16.48(2) ( A ̊ ) , c = 25.205(5) A ̊ , γ = 120°, hexagonal, space group R3̄. The organic solvent molecules were characterized also by IR, 1H NMR spectra. Weak interaction existed between the organic solvent and the heteropoly acid in the secondary structure. The novel compound showed different behaviours in solubility, oxidizability and photosensitivity in comparison with classical dodeca heteropolyacid of molybdenum and tungsten.
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