Abstract
Herein, ZrSiO4/B2O3/Mg/C system was used to synthesize a ZrB2-based composite by means of a high energy ball milling process. A mechanically induced self-sustaining reaction was achieved in this system. A nanocomposite powder of ZrB2–SiC–ZrC was prepared with an ignition time of approximately 6min of milling. The role of the stoichiometric amounts of B2O3 and carbon was investigated to clarify the governing mechanism for the formation of the product.
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