Abstract
The complexes K2MF5H2O can be devided into two structurally different groups. The dehydration of these compounds has been studied by thermogravimetry, differential thermal analysis and differential scanning calorimetry. It was shown that thermal analysis can not be used to distinguish between coordinated and structural water. In the series of compounds with coordinated water the DTA peak temperatures as well as dehydration enthalpies can be correlated to the crystal field stabilization energy.
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