Abstract
AbstractA procedure for the preparation of anhydrous titanium acetate is given. The yellow colored product has the formula Ti(C2H3O2)4 · 2 (CH3COOH. The reaction between TiCl4 and 1–4 dioxane resulted in the formation of titanium (IV) tetrachloro monodioxanate. This yellow compound was found to decompose at about 190°C. Partial hydrolysis of this compound resulted in the formation of titanium (IV) dichloro dihydroxy monodioxanate, a white compound. The latter complex was soluble in acetone, ethyl ether, water, and decomposed when heated above 300°C.
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