Abstract
The preparation of metalla-sulphur-nitrogen and metalla-selenium-nitrogen complexes from reactions in liquid ammonia is described. For example, reaction of PtCl2(PR3)2 with [S4N3]Cl in liquid ammonia yields Pt(S2N2)(PR3)2. Similar reactions with SOCl2 SO2Cl2 and SeCl4 give complexes containing NSO-, [SO2(NH)2]2- and Se2N22- ligands respectively.
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