Abstract
Abstract Two complexes, [Co(NO2)(acac)2(P)](acac=acetylacetonate ion, P=PBu3, PBu2Ph, PMe2Ph, and PMePh2) and [Co(NO2)2(acac)(PMe2Ph)2], were prepared by a reaction between Na[Co(NO2)2(acac)2] and phosphines. The geometrical structures were determined on the basis of the 1H NMR, electronic, and IR spectra. A cis(NO2,P) configuration was assigned to [Co(NO2)(acac)2(P)], and a trans(P,P) configuration, to [Co(NO2)2(acac)(P)2].
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