Abstract
ABSTRACT Precipitation of the secondary phase is a key factor that influences the strengthening effect of nickel-based superalloy. The precipitation behaviours of the M23C6 carbide and γ′-Ni3(Ti, Al) phase in Inconel 617B alloy aged at 700°C for different times were studied by scanning electron microscopy, transmission electron microscopy and atom probe tomography. Plate-like carbide nucleated in the interior of grain and irregular shape carbide precipitated at grain boundary respectively during the early stage of ageing. γ′ particle co-precipitated around carbide is a common microstructure feature during ageing for 5–160 h. After ageing for 160 h, γ′ phase is the main secondary phase. The carbide only distributes on the grain boundary, high density γ′ particle homogeneously distributes in the matrix after a longer ageing time. Elemental partitioning to the secondary phases and composition profiles across different phases was quantitatively analysed. Enrichments of Ti and Al at the carbide/γ interface are directly observed, which act as the nucleation site of γ′ particles during ageing. Enrichments of B, Si and Co at different interfaces are also detected. Based on the experimental results, the precipitation mechanisms of γ′ particles and carbide were discussed.
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