Abstract
Both mercuration and bromination have been used for the polarographic analysis of isopropenyl esters in aqueous solutions. For mercuration, no disadvantages were found in comparison with the established methods [4,5] for the estimation of vinyl esters in methanol, due to either the lower rate of mercuration [5,22] or the expected lower stability of the depolariser formed in aqueous solution, the hemiacetal mercuric acetate addition product. At concentrations below 10 −2 mol l −1, acetone did not interfere [38] with the determinations.
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