Abstract
AbstractYellow crystals of the phosphorus selena bromide α‐P4Se3Br2 [monoclinic, C2/c, Z = 8, a = 12.724(3) Å, b = 14.732(3) Å, c = 12.553(3) Å, β = 116.60(3)°] were obtained from the reaction of P4Se3 and bromine at 80 °C in sealed glass ampoules. The crystal structure features discrete molecules of the formula α‐P4Se3Br2 according to the well‐known α‐form of P4Ch3I2 molecules (Ch = S, Se).
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