Abstract
Antimony-121 Mössbauer spectroscopy, powder X-ray diffraction, and energy dispersive X-ray analysis show that solid solutions of <4% antimony in titanium(IV) oxide contain only antimony(V) in the rutile structure with lattice parameters similar to those of pure titanium dioxide. The results are in distinct contrast to those recently reported (N. Morita, T. Endo, T. Sato, and M. Shimada, J. Solid State Chem. 68, 106 (1987)) from a study of the same system by powder X-ray diffraction, atomic absorption spectrophotometry, and X-ray photoelectron spectroscopy.
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