Abstract
The molecular structure of bis(dipivaloylmethanato)copper(II) has been determined by sector-microphotometer gas electron diffraction. The experimental data are consistent with a monomeric square-planar structure with ∠OCuO = 93.7 ± 0.7°. The structural parameters are as follows: r g ( CuO) = 1.916 ± 0.005 A ̊ , r g ( CO) = 1.284 ± 0.009 A ̊ , r g ( CC ring ) = 1.399 ± 0.023 A ̊ , r g ( CC t ) = 1.581 ± 0.022 A ̊ , r g ( C tC m ) = 1.512 ± 0.006 A ̊ , r g ( C mH ) = 1.112 ± 0.009 A ̊ . The amplitudes of vibration have been calculated by a normal vibration treatment using a valence force field.
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