Abstract

The “mild thiolation” is a term coined specifically for the oxidation of suitable CH-acidic substrates with elemental sulfur in the presence of a base and a dipolar aprotic solvent. Dithiocarboxylates are formed under mild reaction conditions as products which, due to their increased reactivity toward nucleophiles, allow various transformations. The focus of this work is particularly the class of thioamides and their great benefits for the synthesis of heterocycles.

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