Abstract
AbstractThe electron impact‐induced fragmentation of benzoin methyl ether gives rise to the formation of an m/e 91 fragment ion which is not present in the mass spectrum of benzoin. Deuterium and 13C labelling, as well as low energy experiments, revealed that this ion is formed from [M – benzoyl]+ by transfer of both the ether methyl group and the hydrogen atom from the α‐position to the adjacent phenyl ring followed by loss of CO and hydrogen.
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