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Abstract
A measurement technique enabling the determination of low uranium concentration utilizing system used for time resolved laser induced fluorescence spectroscopy (TRLFS), based on a commercially available kinetic phosphorescence analysis method has been developed. The effect of the matrix, complexing agent, and the level of acidification on the fluorescence spectra and integral intensity was studied. The method is highly influenced by the sample matrix; particularly if different starting uranium salts are in the calibration solutions and in the samples. In the initial study of these effects, TRLFS measurements have been used in order to clarify this behavior.
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