Abstract

The requirement of large, recrystallized, highly elongated grains is of primary importance to the development of suitable high temperature properties in oxide dispersion strengthened superalloys. In the present study the recrystallization behavior of MA 6000E, a recently developed Y2O3 strengthened superalloy produced by mechanical alloying, was examined using transmission and replication microscopy. Gradient and isothermal annealing treatments were applied to extruded and hot rolled product. It was found that conversion from a very fine (0.2 μm) grain structure to a coarse (≅10 mm) grain structure is controlled by the dissolution of the gamma prime phase, while grain shape was controlled primarily by the thermal gradient. The fine uniform oxide dispersion appeared to have only a secondary influence in determining the grain shape as columnar grains could be grown transverse to the working direction by appropriate application of the thermal gradient.

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