Abstract
Summary A scheme is described for the identification of all the sulphonamide drugs at present available in this country. The six stages of the process are simple and rapid operations involving no unusual reagents or apparatus: (i) purification of the crude material by charcoal treatment in acetone solution, followed by melting-point determination. (ii) preliminary identification as a sulphonamide compound by decomposition with soda-lime. (iii) detection of free primary amino group by condensation with furfural. (iv) simple crystal tests based on precipitation from ammonia solution by acetic acid vapour. (v) vanillin confirmatory test for sulphamerazine and sulphadimidine. (vi) mixed melting-point determination.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
