Abstract

A new detection system based on an array of 3He tubes and innovative fast detection electronics has been installed on the high-intensity small-angle neutron scattering (SANS) diffractometer KWS-2 operated by the Jülich Centre for Neutron Science (JCNS) at the Heinz Meier-Leibnitz Zentrum in Garching, Germany. The new detection system is composed of 18 eight-pack modules of 3He tubes that work independently of one another (each unit has its own processor and electronics). To improve the read-out characteristics and reduce the noise, the detection electronics are mounted in a closed case on the rear of the 3He tubes' frame. The tubes' efficiency is about 85% (for λ = 5 Å) and the resolution slightly better than 8 mm. The new detection system is characterized by a dead-time constant of 3.3 µs per tube and an overall count rate as high as 6 MHz at 10% dead-time loss. Compared with the old detector this is an improvement by a factor of 60. The much higher count rate will shorten the measurement times and thus increase the number of experiments possible in a given time period by the optimal use of the high flux of up to 2 × 108 n cm-2 s-1 at the sample position. Combined with the event-mode operation capability, this will enable new scientific opportunities in the field of structural investigations of small soft-matter and biological systems. The implementation of the detector in the high-intensity concept on KWS-2, its characterization and its performance based on test experiments are reported in this paper.

Highlights

  • The small-angle neutron scattering (SANS) diffractometer KWS-2, operated by the Julich Centre for Neutron Science (JCNS) at the Heinz Maier-Leibnitz Zentrum (MLZ) in Garching, Germany, is dedicated to the investigation of mesoscopic multi-scale structures and structural changes due to rapid kinetic processes in soft condensed matter and biophysical systems

  • Following detailed simulations by McStas (Willendrup et al, 2004) using a realistic model for the cold neutron source (CNS) of the FRM II reactor (Zeitelhack et al, 2006) and the real parameterization of the neutron guide system upstream of KWS-2, it was shown that, by tilting a selector designed for a resolution of Á/ = 10% over an angle of À10 with respect to the beam axis, a gain in intensity based on the resolution relaxation up to Á/ = 20% can be obtained

  • As the new detection system is composed of several eight-pack units that work independently of one another, the performance of one detector unit and that of one single tube were tested in advance on KWS-2 in a prototyped eight-pack unit of 3He

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Summary

Introduction

The small-angle neutron scattering (SANS) diffractometer KWS-2, operated by the Julich Centre for Neutron Science (JCNS) at the Heinz Maier-Leibnitz Zentrum (MLZ) in Garching, Germany, is dedicated to the investigation of mesoscopic multi-scale structures and structural changes due to rapid kinetic processes in soft condensed matter and biophysical systems. KWS-2 provides a very high neutron flux on the sample (Fig. 1) This is a result of the combination of a neutron guide system that was specially designed to transport high intensity to the instrument (Radulescu et al, 2012) and a versatile velocity selector (Astrium GmbH) that enables easy selection between a wavelength spread of 10 and 20%, depending on whether the specific scientific experiment demands either an improved resolution, Á/ = 10%, or a high intensity, Á/ = 20%. It is very challenging to resolve such weak scattering signals, owing to the requirements regarding the counting rate and stability in time of the pixel response of the detection system These factors are dictated by the specific conditions of an experiment, especially in the field of biology. We report the implementation of the new detector in the highflux concept of the instrument, the characterization and adjustment of the detector, and its performance as proven in measurements of some chosen samples representative of the scientific topics developed on the instrument

The flux conditions on KWS-2
Detector characterization
Counting rate and dead time
Stability of the pixel response
Detector performance
Wavelength and intensity calibration
Two-dimensional scattering patterns and Qmax
Event-mode option
Size standard samples
Biological samples
Findings
Conclusions
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