The formation and dissolution mechanisms of Laves phase in Inconel 718 fabricated by selective laser melting compared to directed energy deposition and cast

Abstract

In this study, we explain why the amount of Laves phase in Inconel 718(IN718) manufactured by selective laser melting (SLM) unexpectedly increases under extremely rapid solidification and clarify its distinct dissolution behavior during heat treatment based on a comparative analysis of laser directed energy deposition (L-DED)-built and cast IN718. Compared with the cast and L-DED, SLM has much higher cooling rate, which greatly improves the dendrite growth rate and the solute trapping during the solidification process of molten pool. Thus, more Nb atoms are trapped in the matrix, and less Nb atoms are expelled to form inter-dendritic Laves phase in SLM-built IN718. However, the volume fraction of Laves phase is the highest in SLM-built IN718, which is attributed to the lower Nb concentration in the Laves phase and few Nb-rich region. During homogenization treatment, the dissolution of Laves phase is controlled by three-dimensional diffusion process at the early stage, and then is mainly controlled by the interface reaction process. After homogenization, there are still many tiny carbides, oxides, and nitrides undissolved both along the grain boundaries and inside the grains.