Abstract
The paramagnetic cuboidal clusters [Mo3(GaCl)(μ3-S)4(dppe)3Cl3] and [W3(GaBr)0.81(μ3-S)4(dppe)3Br3] were synthesized by treatment of the corresponding triangular clusters [M3S4(dppe)3X3]X with [Ga(η5-C5Me5)]6.
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