Abstract
We conducted an x-ray study of crystals of bis(O,O'-diisopropyldithiophosphato)-bis-~(O,O'-dialkylperthiophosphato)diosmium obtained by reacting 0.22 g of ammonium hexachloroosmiate(IV) with 0.46 g of ammonium O,O'-diisopropyldithiophosphate (the mixture was kept for 6 months in i0 ml of water in the absence of O=; subsequently the precipitate was washed with water, dried, and recrystallized from mesitylene).
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