Abstract
The nickel(II) and cobalt(II) complexes have been synthesized and charactetized as the first examples of metal complexes of a 14-membered cyclidene. [(2,3,16,17,19,29-Hexamethyl-3,1(,20,23,26,29-hexaazabicyclo[16.6.6]tiaconta-1,17,19,23,25,29-hexaene-k 4 N 20,23,26,29 )nickel(II)] hexafluoxophosphate, NiC 30 H 52 N 6 P 2 F 12 tallized in the orthorhombic space group Pna2 1 .
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