Abstract

Improved device for the implementation of extraction processes using supercritical fluids (SCF), which allows to achieve a constant predetermined pressure in the cell and to eliminate multiple control of the SCF flow rate due to the installation of a chiller that provides increased heat transfer performance and minimal inertia of coolant temperature fluctuation. To assess the reliability of the results obtained at the facility, verification measurements of the solubility of anthracene in supercritical carbon dioxide (SC-CO2) were carried out at T = 423 K and P = 10 - 20 MPa. The results are in good agreement with published data. The methodology for expressing measurement uncertainty is described in detail taking into account parameters that contribute to the uncertainty based on the calculation formula for calculating the solubility of anthracene and the measurement uncertainty of the specified parameters.

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