Abstract
In the present work, an efficient metal organic framework/graphene oxide (MOF-801/GO) sorbent was fabricated and employed for the detection of organosulfur pesticides (OSPs) in real samples using gas chromatography-flame photometric detection (GC-FPD). The optimal extraction parameters for the suggested solid-phase extraction (SPE) include sorbent amount (60 mg), extraction solvent (acetonitrile) and extraction time (5 min). The linear dynamic ranges and detection limits for organosulfur pesticides (OSPs) samples under above extraction conditions were ranged from 0.5 to 300 μg L−1 and 0.1–1.1 μg L−1, respectively. Moreover, the proposed SPE/GC-FDP method was applied for the analysis of pesticides in different real environmental water and soil samples. The obtained recoveries of the analytes in were between 92.0 and 106.8% and relative standard deviation (RSD) values were lower than 9.2%. The application of the MOF-801/GO as a sorbent in dSPE of OSPs analytes showed to be reliable, fast and sensible methodology for pesticides monitoring in different environmental samples.
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