Abstract
Cyclic voltammetry and potential step techniques have been used to study the electrodeposition of indium metal from 1 mol dm −3 potassium chloride, pH 2–4.5, onto a vitreous carbon electrode. It is confirmed that the In/In 3+ couple is fast in chloride media and the nucleation and growth of the indium phase is discussed. It is shown that instantaneous nucleation occurs at an overpotential of only a few mV and that the growth of the nuclei is three dimensional.
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